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back To Main VACUUM TECHNOLOGIES
Basic Terms of Vacuum
Metrology
Today, the
total range of vacuum pressure accessible to measurement extends from
atmospheric pressure (about 1000 mbar (750 Torr))
down to 10-12 mbar/Torr, i.e. it extends over 15 powers of ten. The
instruments used for measuring the pressure within this wide range are called
vacuum gauges. For physical reasons it is not possible to create a single
vacuum sensor through which it might be possible to perform quantitative
measurements within the entire pressure range. Therefore, a variety of
different vacuum gauges are available, each with their own characteristic
measurement range which commonly extends over several powers of ten. A
difference is made between direct and indirect pressure measurements. In the
case of direct (or absolute) pressure measurements, the readings obtained
through the vacuum gauge are independent of the type of gas and the pressure
which is to be measured. Common are so-called mechanical vacuum gauges where
the pressure is determined directly by recording the force acting on the
surface of a diaphragm. In the case of so-called indirect pressure measurements
the pressure is determined as a function of a pressure dependant property of
the gas (thermal conductivity, ionization probability, for example). These
properties do not only depend on the pressure, but also on the molar mass of
the gases.
For this reason, the pressure readings
obtained through vacuum gauges which rely on indirect pressure measurements,
depend on the type of gas. The readings usually relate to air or nitrogen as
the measurement gas. For the measurement of other vapors or gases the
corresponding correction factors must be applied.
Vacuum Gauges where
the Pressure Readings are Independent of
the Type of Gas (Mechanical Vacuum Gauges)
BOURDON Vacuum Gauge
The
inside of a tube which is bent into a circular arc (the so-called Bourdon tube)
is connected to the vacuum system. Due to the effect of the external atmospheric
pressure, the end of the tube bends more or less during the evacuation process.
This actuates the pointer arrangement which is attached to this point. The
corresponding pressure can be read off on a linear scale. With Bourdon gauges it
is possible to roughly
determine pressures between 10
mbar (7.5 Torr) and atmospheric pressure.
Capsule Vacuum Gauge
This vacuum
gauge contains a hermetically sealed, evacuated, thin-walled diaphragm capsule
which is located within the instrument. As the vacuum pressure reduces, the
capsule bulges. This movement is transferred via a system of levers to a
pointer and can then be read off as the pressure on a linear scale.
Diaphragm Vacuum Gauge
In the case
of the diaphragm vacuum gauge which is capable of absolute pressure
measurements, a sealed and evacuated vacuum chamber is separated by a diaphragm
from the vacuum pressure to be measured. This serves as the reference quantity.
With increasing evacuation, the difference between the pressure hich is to be measured and the pressure within the
reference chamber becomes less, causing the diaphragm flex. This flexure may be
transferred by mechanical means like a lever, for example, to a pointer and
scale, or electrically by means of a strain gauge or a bending bar for conversion
into an electrical measurement signal.
The measurement range of such diaphragm vacuum gauges extends from 1 mbar (0.75
Torr) to over 2000 mbar (1500 Torr).
Capacitance Vacuum Gauge
The pressure
sensitive diaphragm of these capacitive absolute pressure sensors is made of Al2O3 ceramics. The
term “capacitive measurement” means that a plate capacitor is created by the diaphragm with a
fixed electrode behind the diaphragm. When the distance between the two plates of this
capacitor changes, a change in
capacitance will result. This change,
which is proportional to the pressure, is then converted into a corresponding
electrical measurement signal. Here too, an evacuated reference chamber serves
as the reference for the pressure measurements. With capacitance gauges it is
possible to accurately measure pressures from 10-5
mbar/Torr
to well above
atmospheric pressure, whereby different capacitance gauges having diaphragms of
different thickness (and therefore sensitivity) will have to be used.
Vacuum Gauges
where the Pressure Readings Depend of the Type of Gas
Thermal Conductivity Gauge (Pirani)
This
measurement principle utilizes the thermal conductivity of gases for the
purpose of pressure measurements in the range from 10-4
mbar/Torr
to atmospheric pressure. Today, only the principle
of the controlled Pirani gauge is used by LEYBOLD in order to attain a quick
response.
The filament
within the gauge head forms one arm of a Wheatstone bridge. The heating voltage
which is applied to the bridge is controlled in such a way, that the filament
resistance and thus the temperature of the filament remains constant regardless
of the quantity of heat given off by the
filament. Since the heat transfer from the filament to the gas increases
with increasing pressures,
the voltage across the bridge is a measure of the pressure.
Improvements with regard to temperature compensation have resulted in stable
pressure readings also in the face of large temperature changes, in particular
when measuring low pressures.
Cold Cathode Ionization Vacuum Gauge
(Penning)
Here the
pressure is measured through a gas discharge within a gauge head whereby the gas discharge is
ignited by applying a high tension. The resulting ion current is output as a
signal which is proportional to the prevailing pressure. The gas discharge is
maintained also at low pressures with the aid of a magnet. New concepts for the
design of such sensors permit safe and reliable operation of these socalled Penning ensors
in the pressure range from 10-2 to 1 x 10-9 mbar/Torr.
Hot Cathode Ionization Vacuum Gauge
These
sensors commonly use three electrodes. A hot cathode emits electrons which
impinge on an anode. The gas, the pressure of which is to be measured, is thus
ionized. The resulting positive ion current is detected through the third
electrode - the so-called ion detector - and this current is used as the signal
which is proportional to the pressure. The hot cathode sensors which are mostly
used today, are based on the Bayard-Alpert principle.
With this electrode arrangement it is possible to make measurements in the
pressure range from 10-10 to 10-2 mbar/Torr. Other electrode arrangements permit access to a
higher range of pressures from 10-1
mbar/Torr down to 10-10
mbar/Torr. For the measurement of pressures below 10-10
mbar/Torr
so-called extractor ionization sensors after Redhead are employed. In extractor ionization
gauges the created ions are focused onto a very thin and short ion detector.
Due to the
geometrical arrangement of this system, interfering influences such as X-ray
effects and ion desorption can be almost completely
eliminated. The extractor ionization gauge permits pressure measurements in the
range from 10-4 to
10-12
mbar/Torr.
Selection
of the Right Vacuum Gauge
When selecting a suitable instrument for
pressure measurements, the pressure range is not the only critera.
The operating conditions for the instrument play an important part. If, for
example, there
is the risk of excessive contamination, vibrations, or if air inrushes are to
be expected etc., the instrument must be
rugged enough. Thus for industrial applications diaphragm gauges, controlled thermal conductivity gauges as
well as cold cathode ionization gauges after
Penning are strongly recommended. Precision instruments are very often
quite sensitive to rough operating conditions. These should therefore only be used while observing the
corresponding applications information.
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